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  • BSI
    PD IEC TS 62607-6-13:2020 Nanomanufacturing. Key control characteristics - Graphene-based material. Oxygen functional group content: Boehm titration method
    Edition: 2020
    $430.42
    / user per year

Description of PD IEC TS 62607-6-13:2020 2020

This part of IEC TS 62607 establishes a standardized method to determine the chemical key control characteristic

  • oxygen functional group content for powder consisting of graphene-based material like graphite oxide, graphene oxide, reduced graphene oxide and other types of functionalized graphene by

  • Boehm titration method.

In this document, the measured functional groups are carboxyl groups (also in the form of their cyclic anhydrides), lactone groups, hydroxyl groups and reactive carbonyl groups. Oxygen functional groups that exhibit no reactivity such as epoxides cannot be measured.

The oxygen functional group content is derived by the difference between NaHCO3, Na2CO3, NaOH and C2H5ONa consumption of dispersed graphene powders.

  • The oxygen functional group content determined according to this document is listed as key control characteristic in the blank detail specification for graphene IEC 62565-3-1.

  • The method is applicable for graphene powder and graphene related carbon 2D materials such as graphene oxide powder and reduced graphene oxide powder, which can be separated from the water and ethanol by centrifugation or filtration. This document is not applicable for sulfonate modified graphene.

  • In this document, the lower limits of detection (Annex C) for carboxyl groups, lactone groups, hydroxyl and carbonyl are 0,015 mmol/g, 0,037 mmol/g, 0,014 mmol/g, and 0,072 mmol/g, respectively.

  • This document targets graphene manufacturers and downstream users to guide their material design, production and quality control.



Standard NumberPD IEC TS 62607-6-13:2020
TitleNanomanufacturing. Key control characteristics - Graphene-based material. Oxygen functional group content: Boehm titration method
StatusDefinitive
Publication Date2020-11-04
Identical National Standard OfIEC TS 62607-6-13:2020/COR1:2020
CorrectsPD IEC TS 62607-6-13:2020
DescriptorsNanomaterials, Oxygen, Powder, Manufacturing, Nanotechnology
ICS07.120 Nanotechnologies
CommitteeNTI/1
ISBN978 0 539 15824 3
PublisherBSI
Pages36



About BSI

BSI Group, also known as the British Standards Institution is the national standards body of the United Kingdom. BSI produces technical standards on a wide range of products and services and also supplies certification and standards-related services to businesses.
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